[A modified method for the microdetermination of citric acid].
نویسنده
چکیده
An investigation of the different steps in the method of Weil-Malherbe & Bone (1949), as modified by Taylor (1953), has led to an altered procedure for citric acid determination, with increased sensitivity and accuracy. The main modifications involved are the use of (i) a higher concentration of sulphuric acid during the formation of pentabromoacetone, and (ii) a thiourea-borax-sodium sulphide solution in place of 2 % sodium sulphide.
منابع مشابه
A colorimetric method for the determination of citric acid in blood and plasma.
As early as 1897 the oxidative bromination of citric acid to form a brominated acetone derivative, presumably principally pentabromoacetone, was adapted to the quantitative determination of citrate (1). Most subsequent procedures have been based on the same reaction. Among the more recently described procedures are those of Pucher (2) and of Goldberg and Bernheim (3). These methods, with minimu...
متن کاملبررسی منحنی عبور در فرآیند جذب سطحی اسید سیتریک توسط رزین آنیونی و ارایه یک مدل ریاضی
In this research paper, an experimental breakthrough curve for citric acid in an adsorption recovery process was determined by an ion-exchange resin in 20, 35, 55 °C. Also, a mathematical model for breakthrough curve was presented. Among ion exchange resins that have been experienced, many weak and strong basic anionic resins are available such as, IRA-92, IRA-93, IRA-420 and IRA-458 and all of...
متن کاملDetection of Ascorbic Acid in Biological Samples by a New Modified Glassy Carbon Electrode
The present work describes the construction of a new modified electrode by casting the appropriate mixture of a metallocene, which has been introduced in the experimental part, as a mediator at the surface of glassy carbon (GC) electrode. The proposed modified GC electrode was used for the determination of ascorbic acid (AA) in phosphate buffer (PB) solution (pH = 4.0). When compared to bare GC...
متن کاملThermal Analysis of Acrylonitrile/Acrylic Acid Copolymer Dendrigrafted with Citric Acid
Thermal analysis of acrylonitrile/acrylic acid P(AN/AA) copolymer films containing 5%, 10% and 20% acrylic acid dendrigrafted with citric acid (CA) is examined using differential scanning calorimetry (DSC) with various heating rates, thermogravimetry (TGA) and derivative thermogravimetric analysis (DTG). Also, the effect of carboxylic acid on thermal stabilization of the P(AN/AA) copolymers, wh...
متن کاملSynthesis and Characterization of PbTiO3 Nanopowders by Citric Acid Gel Method
High purity lead titanate nanopowders in tetragonal form have been successfully prepared bycitric acid gel method using lead nitrate and tetra-n-butyl titanate as Pb and Ti sourcesrespectively and citric acid as complexing reagent. The precursors were calcined at varioustemperatures ranging from 450 °C to 600 °C for 2 h. Fourier Transform InfraredSpectroscopy (FT-IR), X-ray diffraction (XRD) an...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید
ثبت ناماگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید
ورودعنوان ژورنال:
- The Biochemical journal
دوره 60 4 شماره
صفحات -
تاریخ انتشار 1955